SBIR/STTR Research Award

SYNTHESIS OF CADMIUM SULFIDE

Award identifier db75179387bee392ebed453249865d70e1a4c416c9a8632f9af1425d1292d0deAwarding agency Department of Defense · Army

Award amount

$50,000

Program and phase

SBIR · Phase I

Award year

1991

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Award details

Awarding agency
Department of Defense
Branch
Army
Recipient company
Microgravity Systems Inc.
Proposal award date
Not reported
Contract end date
Not reported
UEI
Not reported
Solicitation number
Not reported
Topic code
Not reported

Research abstract

IN PHASE I, A SYSTEMATIC AND COMPLETE INVESTIGATION ON THE SYNTHESIS OF CADMIUM SULFIDE WILL BE CONDUCTED. CADMIUM SULFIDE (CDS) WILL BE SYNTHESIZED BY TWO METHODS: 1. SPONTANEOUS REACTION BETWEEN DIMETHYLCADMIUM AND HYDROGEN SULFIDE, AND 2. REACTION OF CADMIUM AND SULFUR ELEMENTS BY VAPOR DEPOSITION. THE CDS POWDER OBTAINED FROM THESE TWO TECHNIQUES WILL BE HEAT-TREATED BY BAKING OUT AT ELEVATED TEMPERATURES UNDER VACUUM CONDITION TO ADJUST ITS STOICHIOMETRY. VARIOUS ANALYSES, INCLUDING ATOMIC ABSORPTION SPECTROSCOPY, SPARK SOURCE MASS SPECTROSCOPY AND ENERGY DISPERSION OF X-RAY ANALYSIS, WILL BE PERFORMED ON EACH BATCH OF CDS TO CHARACTERIZE THE PURITY AND STOICHIOMETRY. THE OPTIMAL SYNTHESIS PARAMETERS WILL BE ESTABLISHED.

Technology keywords

Not reported

Agency intelligence

Department of Defense

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