SBIR/STTR Research Award

HIGH-RESOLUTION PREPARATIVE LIQUID CHROMATOGRAPHY

Award identifier edcc12a95ab71592a1cf4fd483689f1a9623b307148f961a554b04636abbb4b3Awarding agency National Science Foundation

Award amount

$50,000

Program and phase

SBIR · Phase I

Award year

1990

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Award details

Awarding agency
National Science Foundation
Branch
Not reported
Recipient company
Ionics International, Inc.
Proposal award date
Not reported
Contract end date
Not reported
UEI
Not reported
Solicitation number
Not reported
Topic code
Not reported

Research abstract

WE PROPOSE TO DESIGN, EVALUATE, AND CONSTRUCT A NEW TYPE OF CHROMATOGRAPHIC SYSTEM CAPABLE OF SEPARATING GRAM QUANTITIESOF PEPTIDE HORMONE AND OTHER SUBSTANCES WITH HIGH RESOLUTION. THE HEART OF THE SYSTEM WILL BE AN EXTRUDED MULTI-CHANNEL CERAMIC BLOCK. SUCH BLOCKS ARE COMMERCIALLY AVAILABLE WITH SEVERAL THOUSAND PARALLEL CHANNELS OF IDENTICAL DIMENSION. THIS IS EQUIVALENT TO USING THOUSANDS OF IDENTICAL CHROMATOGRAPHIC COLUMNS IN PARALLEL. THUS, THERESOLVING POWER OF A CAPILLARY COLUMN CAN BE COMBINED WITH THE HIGHER SAMPLE CAPACITY OF A PREPARATIVE-SCALE COLUMN. DURING PHASE I WE PROPOSE TO DEVELOP A METHOD FOR DRY-PACKING THE CERAMIC BLOCKS, CONSTRUCT AN ENTIRE CHROMATOGRAPHIC SYSTEM, AND EVALUATE THE SYSTEM USING FLUORESCENT HYDROCARBONS. ALTERNATIVE MULTI-CHANNEL COLUMNSWILL ALSO BE EVALUATED.

Technology keywords

Not reported

Agency intelligence

National Science Foundation

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